Mantis 5000 Especificaciones descargar pdf (Pagina 46)

Sample Preparation Using the PCH-150 Powder Cell Holder

Figure 40. An exploded view of the powder cell.

1. Disassemble the powder cell holder. DO NOT disassemble the reference cell holder.

Place the front cover onto the flat surface of a balance scale, face down, and load the

quartz window into the cover.

2. Record the weight of the two sample holder components.

3. Load a portion of the sample into the powder cell cavity over the quartz window.

Gently tap the side of the holder against the work table, or use a spatula to smooth the

surface of the sample. Repeat this loading process until the desired sample depth or

sample weight is achieved.

4. Record the weight on the balance scale and calculate the total weight of the powdered

sample.

5. Estimate the average height of the sample by measuring the distance from the sample

to the top surface of the container.

6. Load the plunger and spring over the sample and screw the body over the entire

assembly. Screw the pieces together snugly, but do not apply excessive force.

7. Examine the surface around the sample holder for any loose sample material that may

have spilled out of the sample holder cavity. Weigh the spilled powder and make

corrections to your calculation in Step 4.

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Mantis 5000 Especificaciones Pagina 46